§761.395. A validation study.
40 C.F.R. § 761.395
Decontaminate the following prepared sample surfaces using the selected testing parameters and experimental conditions. Take a standard wipe sample of the decontaminated surface.
At least one uncontaminated surface. The surface levels of PCBs on the uncontaminated surface must be <1 µg/100 cm 2.
At least seven contaminated surfaces.
Select applicable method(s) from the following list to extract PCBs and determine the PCB concentration from the standard wipe sample collection medium: SW-846 Method 3540C, Method 3550C, Method 3541, Method 3545A, Method 3546, or Method 8082A (all standards incorporated by reference in § 761.19). Modifications to the methods listed in this paragraph or alternative methods not listed may be used if validated under subpart Q of this part.
Report all validation study surface sample concentrations on the basis of micrograms of PCBs per 100 cm 2 of surface sampled.
Following completion of the validation study, measurements from the contaminated surfaces must have an arithmetic mean of ≤10 µg/100 cm 2. If the arithmetic mean is >10 µg/100 cm 2, then the validation study failed and the solvent may not be used for decontamination under § 761.79(d)(4) according to the parameters tested.
Notes, amendments, and revision history
Amendments
[63 FR 35473, June 29, 1998, as amended at 88 FR 59696, Aug. 29, 2023]
Source
Source: 63 FR 35473, June 29, 1998, unless otherwise noted.
Authority
Authority: 15 U.S.C. 2605, 2607, 2611, 2614, and 2616 and 42 U.S.C. 6939g.
Source
Source: 43 FR 7156, Feb. 17, 1978, unless otherwise noted.
Amendments
[63 FR 35473, June 29, 1998, as amended at 88 FR 59696, Aug. 29, 2023]